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PC1 post-catalysis C1s Ru3d scan.EMF (21.02 kB)

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PC1 post-catalysis Ni2p scan.EMF (32.11 kB)

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PC1 post-catalysis O1s scan.EMF (14.84 kB)

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PC1 post-catalysis Pd3d scan.EMF (18.95 kB)

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PC1 pre-cat C1s Ru3d scan.EMF (18.91 kB)

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PC1 pre-catalysis C1s Ru3d scan.EMF (23.7 kB)

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PC1 pre-catalysis Ni2p scan.EMF (33.09 kB)

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PC1 pre-catalysis O1s scan.EMF (14.66 kB)

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PC1 pre-catalysis Pd3d scan.EMF (19.7 kB)

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PC2 post-catalysis C1s Ru3d scan.EMF (20.87 kB)

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PC2 post-catalysis Ni2p scan.EMF (32.83 kB)

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PC2 post-catalysis O1s scan.EMF (14.71 kB)

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PC2 post-catalysis Pd3d scan.EMF (18.41 kB)

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PC2 pre-catalysis C1s Ru3d scan.EMF (18.45 kB)

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PC2 pre-catalysis Ni2p scan.EMF (32.84 kB)

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PC2 pre-catalysis O1s scan.EMF (15.06 kB)

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PC2 pre-catalysis Pd3d scan.EMF (18.59 kB)

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PC3 post-catalysis C1s Ru3d scan.EMF (21.66 kB)

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PC3 post-catalysis Ni2p scan.EMF (32.66 kB)

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PC3 post-catalysis O1s scan.EMF (16.1 kB)

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XPS Data: Photoelectrochemical hydrogen evolution using dye-sensitised NiO - Environmental Effects and Photocatalyst Design Considerations

dataset

posted on 2021-06-30, 16:09 authored by Joshua KarlssonJoshua Karlsson, Elizabeth GibsonElizabeth Gibson, Abigail Alice SeddonAbigail Alice Seddon

X-ray photoelectron spectroscopy (XPS) data for the five photocatalysts in this study (PC1-PC5) on mesoporous NiO thin films. XPS data was recorded on a Thermo Scientific K-Alpha instrument. The X-ray source was microfocused monochromatic AlKa, with an energy of 1486.6 eV, voltage = 12 kV, current = 3 mA, and power = 36W (at 400 µm spot size). The emission angle was at zero degrees. Pass energy for the survey regions was 150 eV with a step size of 0.4 eV and high-resolution regions had a pass energy of 40 eV with a step size of 0.1 eV. The samples were mounted on a clean aluminium plater and immobilised using double sided adhesive tape. Spectra were analysed using CasaXPS software (version 2.3.16).